Agilent W DB-5ms Ultra Inert Manuals

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Application Note 6

Key facts

Brand
Agilent
Model
W DB-5ms Ultra Inert
Documents
6
Languages
EN
Last added
2012-07-02

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Agilent J&W DB-5ms Ultra Inert Column Application Note

Agilent J&W DB-5ms Ultra Inert Column Application Note

Application Note 8 pages · 232 KB · EN

This document presents a comparative study on the chromatographic behavior of Agilent J&W DB-5ms Ultra Inert columns versus similar columns from four other manufacturers. The analysis focuses on the inertness required for analyzing very active samples, specifically basic compounds that are prone to tailing due to acidic sites in non-inert columns.

The study utilized an Agilent 6890N GC system to test a mixture of six basic compounds, chlorophenols, organophosphorus pesticides, and aromatic positional isomers. Results demonstrated that the DB-5ms Ultra Inert column provided superior peak shapes with significantly reduced tailing factors compared to the competitor columns, ensuring more accurate and reliable analytical results.

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Agilent W DB-5ms Ultra Inert specifications

Column Length15 m
Column Inner Diameter0.25 mm
Column Film Thickness0.25 µm
Column Part Number122-5512UI
Carrier Gas Flow Rate72 cm/s
Inlet Temperature325 °C
Oven Temperature Range150 to 325 °C
MSD Source Temperature300 °C

Source: Agilent J&W DB-5ms Ultra Inert Capillary GC Column PBDE Analysis Application Note

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Questions answered in these manuals

What specific compounds were used to test the column's performance with basic analytes?

The study analyzed a mixture containing Triethylamine, Pyridine, 4-Methylpyridine, N.N-Dimethylacetamide, 2,4-Dimethylaniline, and Dicyclohexylamine.

From: Agilent J&W DB-5ms Ultra Inert Column Application Note

What is the length of the Agilent J&W DB-5ms Ultra Inert column used in this study?

The column dimensions are 30 m x 0.25 mm x 0.25 um.

From: Agilent J&W DB-5ms Ultra Inert Column Application Note

Which Agilent column is recommended for challenging PBDE analysis?

The document recommends the Agilent J&W DB-5ms Ultra Inert capillary GC column.

From: Agilent J&W DB-5ms Ultra Inert Capillary GC Column PBDE Analysis Application Note

What are the concentration ranges used for BDE calibration?

The study used a range of 0.5 to 250 ng/mL for most BDEs and 2.5 to 1,000 ng/mL for BDE-209.

From: Agilent J&W DB-5ms Ultra Inert Capillary GC Column PBDE Analysis Application Note

What is the lowest concentration of melamine this method can detect in milk?

The limit of detection for melamine in the milk matrix is 0.0025 mg/kg.

From: Agilent Trace-Level Analysis of Melamine in Milk Products on Agilent 7890A/5975C GC/MSD Using a New Agilent J W DB-5ms Ultra Inert Column SampliQ SCX Cartridges Manual

What is the linear concentration range for this melamine analysis method?

The method shows good linearity in the range of 0.025 to 2.000 pg/mL.

From: Agilent Trace-Level Analysis of Melamine in Milk Products on Agilent 7890A/5975C GC/MSD Using a New Agilent J W DB-5ms Ultra Inert Column SampliQ SCX Cartridges Manual