Agilent PLgel 5 pm MIXED-D Manuals

ManualLib has 2 documents for the Agilent PLgel 5 pm MIXED-D (Other Electronics): 2 application notes. Every file can be read online or downloaded as a PDF for free.

Application Note 2

Key facts

Brand
Agilent
Model
PLgel 5 pm MIXED-D
Documents
2
Languages
EN
Last added
2012-06-11

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Agilent PLgel 5 pm MIXED-D Column Application Note for Polyaniline Analysis

Agilent PLgel 5 pm MIXED-D Column Application Note for Polyaniline Analysis

Application Note 2 pages · 539 KB · EN

The document details the use of Agilent PLgel 5 pm MIXED-D columns for analyzing polyaniline, specifically the emeraldine and leucoemeraldine forms. It explains that these columns are ideal for polymers where material above 400,000 MW is unlikely to be present.

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Agilent PLgel 5 pm MIXED-D specifications

Column Dimensions300 x 7.5 mm
Column Efficiency5 um
Flow Rate1.0 mL/min
Injection Volume100 pL
Temperature80 °C
Eluent CompositionNMP + 0.1% (w/v) LiBr

Source: Agilent PLgel 5 pm MIXED-D Column Application Note for Polyaniline Analysis

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Application Note 2

How to use the product for one specific task, with worked examples.

Questions answered in these manuals

What solvents are required for analyzing polar polymers like polyaniline?

Polar organic solvents such as dimethylformamide, dimethyl sulfoxide, and N-methyl-2-pyrrolidinone (NMP) are required.

From: Agilent PLgel 5 pm MIXED-D Column Application Note for Polyaniline Analysis

Why is high temperature GPC often needed for these solvents?

High temperature is needed due to the increased viscosity of these solvents compared to tetrahydrofuran.

From: Agilent PLgel 5 pm MIXED-D Column Application Note for Polyaniline Analysis

Why is toluene used as the eluent instead of THF?

Toluene was chosen because polysiloxanes show very little response in tetrahydrofuran (THF) with a refractive index detector.

From: Agilent PLgel 5 pm MIXED-D Polysiloxane Analysis Application Note

What is the Agilent PLgel 5 pm MIXED-D column designed for?

It is specifically designed for the analysis of polymers, paints, and resin systems where material above 400,000 MW is unlikely to be present.

From: Agilent PLgel 5 pm MIXED-D Polysiloxane Analysis Application Note