Agilent GTA-95 Manuals

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Application Note 2

Key facts

Brand
Agilent
Model
GTA-95
Documents
3
Languages
EN
Last added
2012-06-12

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Agilent Low Level Measurement of Cadmium in Foods Application Note

Agilent Low Level Measurement of Cadmium in Foods Application Note

Application Note 8 pages · 86 KB · EN

This document outlines a procedure for determining cadmium concentrations in animal and plant tissues, including dairy products, grains, fruits, vegetables, and oil seeds. The method is suitable for cadmium concentrations in the range of 0.01-0.3 µg/g. The process involves digesting samples via wet ashing, complexing cadmium with ammonium pyrrolidine dithiocarbamate (APDC), and extracting it into di-isobutyl ketone (DIBK). The organic phase is then stripped with dilute nitric acid, and the resulting aqueous phase is analyzed using Graphite Furnace Atomic Absorption Spectroscopy (GFAAS).

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Agilent GTA-95 specifications

Applicable Cadmium Concentration Range0.01-0.3 µg/g
Instrumentation UsedAgilent GTA 95 with Agilent AA-875
Detection Limit (Solution)Better than 0.0005 mg/mL Cd
Reporting Limit (Grains)0.02 mg Cd/g

Source: Agilent Low Level Measurement of Cadmium in Foods Application Note

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Questions answered in these manuals

What is the suitable range for cadmium concentration in this method?

The method is suitable for cadmium concentration in the range 0.01-0.3 µg/g.

From: Agilent Low Level Measurement of Cadmium in Foods Application Note

Which instruments are used for the analysis?

An Agilent GTA 95 graphite furnace atomizer with autosampler is used with an Agilent AA-875.

From: Agilent Low Level Measurement of Cadmium in Foods Application Note

Which metals are regulated in drinking water according to this note?

Seven metals (As, Ba, Cd, Cr, Pb, Se, and Ag) are regulated in drinking water and may be determined by furnace AA.

From: Agilent AA-975/GTA-95 Application Note: Determination of Toxic Metals in Waters and Wastes by Furnace Atomic Absorption

What matrix modifier was found best for Cadmium analysis?

Ammonium nitrate was found to be the best matrix modifier for Cd.

From: Agilent AA-975/GTA-95 Application Note: Determination of Toxic Metals in Waters and Wastes by Furnace Atomic Absorption