Agilent 4500 ICP-MS Application Note for Determining Vanadium and Nickel in Heavy Oil

About this manual

The document details a method to analyze trace metals, specifically vanadium and nickel, in petroleum products like vacuum gas oil. These metals are critical because they can cause catalyst deterioration during refining processes. The note demonstrates that the Agilent 4500 ICP-MS can perform direct analysis of hydrocarbons by diluting samples with xylenes or other solvents.

What's inside

• Abstract
• Introduction
• Instrumentation
• Sample Preparation
• Operating Parameters
• Results

Frequently asked questions

What metals does this method determine in heavy oil?

The method determines vanadium and nickel in heavy oil.

What is the typical sample uptake rate for the 4500 ICP-MS?

The instrument is typically operated at a sample uptake rate of 0.4 mL/min.

How long does the dry ashing digestion procedure take?

The dry ashing and digestion procedure takes about 17 hours.