Agilent Bond Elut QuEChERS EN Extraction Application Note

This application note describes a simple and rapid extraction procedure for pesticide residues in lemon essential oils. The method uses Agilent Bond Elut QuEChERS extraction and modified dispersive SPE coupled with GC/MS.


Agilent Bond Elut QuEChERS EN Extraction Application Note - cover page
Brand
Agilent
Category
Other
Document type
Application Note
Language
English
Pages
14
File format
PDF
File size
1.2 MB
Published
11 June, 2012
Updated
30 September, 2023
MD5 checksum
9166B1180CA4B82EDF5E6F8382505275

About this manual

This document details a simple and rapid extraction procedure for pesticide residues in lemon essential oils. The method combines Agilent Bond Elut QuEChERS EN Extraction and AOAC dispersive SPE kits with Gas Chromatography/Mass Spectrometry (GC/MS) analysis. It addresses the challenge of detecting chemicals in citrus essential oils, which are extracted from fruit peels and may contain higher concentrations of pesticide residues than the fruit itself.

What's inside

  • Abstract
  • Introduction
  • Reagents and Chemicals
  • Equipments and Materials
  • GC/MS SIM Conditions
  • Sample Preparation
  • Dispersive SPE Cleanup
  • Results and Discussion

Specifications

Internal Standard Concentration100 ng/g
Internal Standard TypeTriphenyl phosphate (TPP)
Centrifuge Speed for Cleanup13,000 rpm

Frequently asked questions

What kits are used for the extraction of volatile and semivolatile pesticides in lemon oil?

The Agilent EN Buffered Extraction kit and Agilent AOAC dispersive SPE kit for fatty and pigmented products are combined.

What is the purpose of this application note?

This document describes a simple and rapid extraction procedure for pesticide residues in lemon essential oils.

What are the US EPA limits for Carbaryl and Chlorpyrifos in citrus oils?

The US EPA limit for Carbaryl is 20 ppm and for Chlorpyrifos is 20 ppm.

What is the concentration of the internal standard solution used in the sample preparation?

The internal standard solution has a concentration of 15 ug/mL.

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