Agilent Ultra Inert Liner Deactivation for Active Compounds Analysis by GC Technical Overview

This document introduces the performance evaluation of Agilent Ultra Inert Liner, which passed Endrin and DDT breakdown and active semivolatiles tests, proving the inertness of Ultra Inert Liner, suitable for the analysis of active compounds


Agilent Ultra Inert Liner Deactivation for Active Compounds Analysis by GC Technical Overview - cover page
Brand
Agilent
Document type
Other
Language
English
Pages
10
File format
PDF
File size
428 KB
Published
05 July, 2012
Updated
30 September, 2023
MD5 checksum
F34BF46FBC416ECBA13B1D028A3C22E4

About this manual

The document presents a technical evaluation of the Agilent Ultra Inert liner's ability to minimize interactions with active compounds during gas chromatography (GC) analysis. It highlights that active sites on inlet liners can cause analyte degradation or adsorption, leading to poor linearity and sensitivity.

Two specific tests were conducted: an Endrin and DDT breakdown test and a USEPA Method 8270 semivolatile active compounds test. The results indicate that the Ultra Inert deactivated liners provide superior inertness compared to proprietary deactivated liners and Restek Siltek deactivated liners, maintaining stability over multiple injections.

What's inside

  • Introduction
  • Experimental
  • Instrumental Conditions
  • Flow Path Supplies
  • Results and Discussion
  • Endrin and DDT Breakdown Test

Frequently asked questions

What is the purpose of deactivating an inlet liner for gas chromatography?

Deactivation minimizes interaction between active analytes and the flow path to prevent degradation or adsorption, which ensures reliable results.

How many injections were performed during the Endrin and DDT breakdown test?

A total of 101 injections were made, including one standard run after an initial cycle of nine solvent injections.

What percentage of Endrin breakdown occurred after the first injection on an Ultra Inert liner?

The first injection delivered a 1.2% Endrin breakdown.

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