Agilent GC/MS Analysis of Trace Fatty Acid Methyl Esters (FAME) in Jet Fuel Using Energy Institute Method IP585

About this manual

The document details an analytical method for measuring trace amounts of Fatty Acid Methyl Esters (FAME) in jet fuel to detect biodiesel contamination. It utilizes Selective Ion Monitoring (SIM) with the Agilent 5975C GC/MS system to improve selectivity and sensitivity within the complex jet fuel matrix.

The note outlines the experimental setup, including specific instrument configurations for the Gas Chromatograph (7890A), Mass Spectrometer (5975C), and Automated Liquid Sampler (7693A). It presents calibration data demonstrating full recovery of FAMEs across a concentration range of 1 to 40 mg/kg with high precision.

What's inside

• Abstract
• Introduction
• Calibration Standards
• Jet Fuel Sample Preparation
• GC/MS Analysis Configuration
• Instrument Conditions
• Results and Discussion

Frequently asked questions

What is the maximum allowed concentration of total FAME in jet fuel according to JIG guidelines?

The Joint Inspection Group has placed a maximum limit of 5 mg/kg (ppm) total FAME in jet fuel.

What concentration range of total FAME was demonstrated in the application note?

Full recovery of FAMEs was achieved across a concentration range of 1 to 40 mg/kg total FAME in jet fuel.

What are the specific concentrations used for the low level calibration standards?

The five low concentration standards used were 2, 4, 6, 8, and 10 mg/kg for each FAME.