Agilent Ultra Inert Liners with Wool Application Note for GC/FID Semivolatile Analysis

The Ultra Inert liners with wool provide superior inertness for accurate analysis of semivolatile analytes by GC/FID, homogeneous sample mixing and evaporation, and maximum column and detector protection.


Agilent Ultra Inert Liners with Wool Application Note for GC/FID Semivolatile Analysis - cover page
Brand
Agilent
Document type
Application Note
Language
English
Pages
8
File format
PDF
File size
514 KB
Published
11 June, 2012
Updated
30 September, 2023
MD5 checksum
46E08F9A4E37B8E02ACE6174C2F95C15

About this manual

The document addresses the historical limitations of glass wool inlet liners, such as active sites causing analyte degradation or adsorption. It introduces Agilent's Ultra Inert deactivation process which effectively treats the large surface area of the glass wool to prevent these issues.

An experimental evaluation was conducted using an EPA 8270 customized standard mix containing difficult compounds like nitrophenols and amines. The study assessed calibration curve linearity, liner-to-liner reproducibility, thermal stability at 330 °C, and injection repeatability on an Agilent GC/FID system equipped with an Ultra Inert deactivated single taper splitless wool liner.

What's inside

  • Introduction
  • Standards and Reagents
  • Instrumentation
  • Results and Discussion
  • Calibration curve linearity
  • Liner to liner reproducibility

Frequently asked questions

What calibration range was used to evaluate the linearity of the Ultra Inert liners with wool?

The evaluation used a calibration range of 2 to 80 ng on column.

What is the minimum signal-to-noise ratio required for the 2 ng on column quantitation limit?

The 2 ng on column quantitation limit requires a signal-to-noise ratio greater than 20.

What is the maximum allowed relative standard deviation for each target analyte according to the EPA 8270 method?

The relative standard deviation for each target analyte should be less than 20%.

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