This application note describes the ultratrace determination of iodine-129 in aqueous samples using the 7700x ICP-MS with oxygen reaction mode.
The document details a method for measuring the radionuclide iodine-129 (I-129) using Inductively Coupled Plasma Mass Spectrometry (ICP-MS). The study utilizes an Agilent 7700x ICP-MS equipped with an Octopole Reaction System (ORS) cell operated in oxygen reaction mode. This setup effectively removes background signals caused by Xenon impurities and polyatomic ions, enabling high-sensitivity detection without sample preparation.
A detection limit of 1.1 ppt was obtained for iodine-129.
No sample preparation is required for aqueous samples.
The total cell gas flow rate was 5.01 mL/min.