Agilent M30_Detection of dioxins furans PCDDs PCDFs in marine sediments by triple quad GCMSMS instrument Manual

A method based on isotopic dilution with low resolution MRM acquisition for higher sensitivity was used for the determination of polychlorinated dibenzo-p-dioxins and dibenzofurans in sediments. The method is accurate and sensitive.

Brand: Agilent
Category: Other Electronics
Document type: Product Leaflet
Language: English
Pages: 1
File format: PDF
File size: 1.6 MB
Published: 05 July, 2012
Updated: 30 September, 2023
Model: 7000 Series
MD5 checksum: 35BF54E93C79DB52BDE280DCAEEFE8AB
PDF: Agilent M30_Detection of dioxins furans PCDDs PCDFs in marine sediments by triple quad GCMSMS instrument Manual PDF

About this manual

This document presents a method for detecting dioxins (PCDDs) and furans (PCDFs) in marine sediments. The analysis was conducted using an Agilent 7000 Series Triple Quad GC/MS/MS instrument with a 60m HP5-MS Ultra Inert capillary column. The study focused on samples collected from six different points off the Lazio coast, Italy, at depths of 0-5cm and 15-20cm.

What's inside

Sample Preparation
GC/MS/MS Method
Method Parameters
Calibration
Results
TEQ Calculation

Specifications

Column	60m HP5-MS Ultra Inert capillary column
Inlet Mode	PTV Pulsed Splitless mode
Injection Volume	4uL
Run Time	40 min

Frequently asked questions

What sample mass and extraction duration were used for the analysis?

The method uses 10g of sediment kept at 40°C for 48 hours before Soxhlet extraction.

What is the total run time for a single analysis?

The complete chromatographic run takes 40 minutes to complete.

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