Agilent Technologies 4000 MS External Ionization User Guide

This manual describes the Varian 4000 MS mass spectrometer external ionization source, introduces the working principle of the external ionization source and how to use the external ionization source


Agilent Technologies 4000 MS External Ionization User Guide - cover page
Brand
Agilent
Document type
User Manual
Language
English
Pages
43
File format
PDF
File size
991 KB
Published
07 June, 2012
Updated
30 September, 2023
Model
4000 MS
MD5 checksum
FEB095E32983D952049E1F2D12305543

About this manual

The document serves as a user guide for the Agilent Technologies 4000 Mass Spectrometer when configured with an external ion source. It details the operational configurations, including External Electron Ionization (EI), Positive Chemical Ionization (PCI), and Negative Chemical Ionization (NCI). The text explains how ions are formed in the external source, transferred to the ion trap analyzer, and analyzed.

The guide provides step-by-step instructions for starting the instrument, performing diagnostic tests, adjusting system temperatures, and conducting mass calibration. It also covers method creation, data acquisition procedures, sample injection via a SampleList, and software interface usage for viewing parameters and activating methods.

What's inside

  • Overview of External Configuration
  • Scan Functions Control MS Processes
  • Steps to Create a Mass Spectrum
  • About External Electron Ionization
  • Starting the Instrument
  • Adjusting and Tuning the 4000 MS
  • Setting Up CI Reagents
  • Preparing a GC/MS Method for Data Acquisition
  • Acquiring Data
  • Editing a Method in Manual Control

Specifications

Document VersionRev. 3
Copyright Period2004-2006

Frequently asked questions

What ionization techniques are supported in the External Configuration?

The system supports electron ionization (EI), negative chemical ionization (NCI), and positive chemical ionization (PCI).

How are ions stored before analysis in this configuration?

Ions are immediately drawn out of the ion source by tuned lenses and directed into an ion trap cavity where they are stabilized by an RF field.

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