Step‑by‑step guide for acquiring and processing HETCOR spectra on a Varian NMR spectrometer.
This guide explains how to set up, acquire, and process heteronuclear correlation (HETCOR) spectra using Varian Vnmr software. It covers sample preparation, basic function buttons, and command usage for 1H and 13C experiments.\n\nThe document also details data processing steps, including 2D Fourier transform, scaling adjustments, and plotting of the final spectrum, and provides final instructions for completing the experiment and returning to routine operation.
| Sample volume | about 0.7 mL |
|---|---|
| TMS concentration | ≤0.1 % |
Press the ABORT ACQ button to halt the acquisition.
Enter the command "movesw" after phasing the 1H spectrum to set up the optimized window.
Enter the command "go" to start the acquisition; do not use "ga".