Agilent Replacing Multiple 50-Minute GC GC-MS/SIM Analyses with One 15-Minute Full-Scan GC-MS Analysis for Nontargeted Pesticides Screening 10x Productivity Gain Manual

Agilent Technologies has introduced a new fast analysis method that can replace the traditional multi-instrument approach with a single 15-minute gas chromatography-mass spectrometry (GC-MS) analysis, reducing the analysis time and improving analysis efficiency. The new method can quickly and accurately detect trace pesticide residues in fruits and vegetables, providing a powerful guarantee for food safety.


Agilent Replacing Multiple 50-Minute GC GC-MS/SIM Analyses with One 15-Minute Full-Scan GC-MS Analysis for Nontargeted Pesticides Screening 10x Productivity Gain Manual - cover page
Brand
Agilent
Category
Other Electronics
Document type
Application Note
Language
English
Pages
18
File format
PDF
File size
1.2 MB
Published
12 June, 2012
Updated
30 September, 2023
Model
7890A
MD5 checksum
28B387795693D9904BF3612B79CBD203

About this manual

This document details a method to improve productivity in pesticide residue analysis by replacing multiple injections with a single injection using an Agilent capillary flow three-way splitter. The system allows simultaneous acquisition of data for Mass Spectrometry (MS), Flame Photometric Detection (FPD), and Electron Capture Detection (ECD).

What's inside

  • Introduction
  • Sample Preparation
  • Capillary Flow Three-Way Splitter
  • Backflush
  • Method Resolution

Specifications

Analysis Time15 minutes
Split Ratio1:1:0.1
Aux Pressure3.8 psi
Splitter Height6.5 cm

Frequently asked questions

How does the three-way splitter enhance productivity?

It splits column effluent proportionally to multiple detectors, allowing two GC detector signals to be acquired together with MS data from one injection.

What is the benefit of the backflush technique?

Backflush removes high boilers from the column faster and at a lower temperature, cutting down analysis time and increasing column lifetime.

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