Agilent Flame Atomic Absorption Spectrometry Fault-Finding Guide

This guide is designed to help analysts troubleshoot common problems with flame atomic absorption spectrophotometers.


Agilent Flame Atomic Absorption Spectrometry Fault-Finding Guide - cover page
Brand
A
Category
Other
Document type
Application Note
Language
English
Pages
6
File format
PDF
File size
61 KB
Published
12 June, 2012
Updated
01 October, 2023
MD5 checksum
B054F0294F33366DEEFBA26143707BFF

About this manual

This document serves as a fault-finding guide for Flame Atomic Absorption Spectrometry (AA) applications. It addresses common operational problems that may arise, helping operators diagnose issues without requiring a service call. The guide covers initial set-up procedures, optimization steps for the flame, and specific troubleshooting sequences for problems like low absorbance.

What's inside

  • Introduction
  • Initial Set-Up
  • Optimization (Flame On)
  • Fault Finding
  • Low Absorbance
  • Nebulizer Blockage
  • Flame Stoichiometry
  • Solution Stability
  • Ionization Suppression

Frequently asked questions

What is the recommended sample uptake rate for a fixed nebulizer?

For a fixed nebulizer, the sample uptake rate should be between 4-6 mL per minute.

What is the recommended spectral bandwidth for the optimum glass bead position test?

The recommended spectral bandwidth for the test is 0.5 nm.

Which elements require a reducing environment for maximum response?

Elements such as barium, molybdenum, and silicon require a reducing environment (fuel-rich flame).

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