Varian 450-GC Gas Chromatograph Application Note SI-01298

This article describes the method of analyzing dissolved gases in transformer oil using gas chromatography. By using a gas chromatograph with a stripper column, the identification and quantification of fault gases in electrical insulating oils can be performed, allowing for early detection of equipment issues.


Varian 450-GC Gas Chromatograph Application Note SI-01298 - cover page
Brand
Agilent
Document type
Application Note
Language
English
Pages
3
File format
PDF
File size
237 KB
Published
12 June, 2012
Updated
29 September, 2023
Model
450-GC
MD5 checksum
85576BBB76C300A31B7702C39B20358A

About this manual

This document details an application for analyzing dissolved gases in electrical insulating oils (TOGA) to detect faults in transformers. The method utilizes ASTM D 3612 Method B principles, employing back flushing of oil and unwanted components.

The procedure uses a Varian 450-GC Gas Chromatograph equipped with a dual channel stripper column oven and a dual channel gas sampling valve (GSV) system. Two separate channels analyze the extracted gases: one using Argon carrier gas to detect lighter gases like hydrogen, oxygen, and nitrogen via TCD; the other using Helium carrier gas to detect carbon gases (CO, CO2, hydrocarbons) via FID with a methanizer.

What's inside

  • Introduction
  • Instrumentation
  • Sample Preparation
  • Conditions
  • Options
  • Results and Discussion
  • Calibration
  • Analysis Methodology

Frequently asked questions

What is the purpose of the Varian 450-GC Gas Chromatograph in this application?

The instrument is used to analyze dissolved gases in transformer oil to identify faults that could degrade the fluid and insulation materials.

What are the carrier gas pressures required for the analysis?

The system requires Helium at 35.5 psi and Argon at 10.4 psi as carrier gases.

What is the temperature setting for the methanizer oven?

The methanizer oven must be set to 400 °C.

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