This document describes a method for using GC/MS to analyze off-flavors in wine
The document outlines a method for analyzing undesirable aroma characteristics, such as cork taint caused by 2,4,6-Trichloroanisole (TCA), geosmin, and other compounds like (+)-fenchone and 2-methyl-iso-borneol. The analysis relies on specific sample preparation steps involving C18 SPE for concentration and SAX SPE for clean-up to remove high molecular weight pigments and free fatty acids.
Geosmin can lead to a distinctive earthy and musty flavor at concentrations as low as 50 ng/L.
The procedure requires a sample size of 5 ug/mL in Acetone.
The temperature increases from 70 °C to 240 °C at a rate of 5 °C per minute.