Agilent Detection Confirmation Quantification Chloramphenicol in Honey Shrimp at Regulatory Levels Using Quadrupole Ion Trap LC/MS Manual

Update: 29 September, 2023

A methodology capable of meeting regulatory requirements has been developed for the determination of chloramphenicol in honey and shrimp. Samples of the two foodstuffs are extracted with Isolute HN-M cartridges and analyzed with both the Agilent 1100 LC/MSD Trap (SL) and the Agilent 1100 LC/MSD (SL) quadrupole with negative mode electrospray ionization. Using deuterated internal standard and one simple sample extraction procedure, both instruments provide a limit of detection at or below 0.1 ppb in both shrimp and honey. Chloramphenicol is a broad range antibiotic that has been banned from foods in the European community and the United States at levels greater than 0.1 ppb.

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Publication date: 12 June, 2012

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PDF Link: Agilent Detection Confirmation Quantification Chloramphenicol in Honey Shrimp at Regulatory Levels Using Quadrupole Ion Trap LC/MS Manual PDF